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PERFUME LOVERS BLOG

MYSTIC ROSES

22/3/2022

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Mystic Roses
by Jan Kusmirek, IPF Chairman UK and Certified Perfumotherapist
The most popular and international fragrance choice of any flower or herb is undoubtedly the Rose. Yet there is no definitive smell of rose for it has so many facets.  The rose because of its bittersweet paradox of smell, beauty and thorns has earned itself a special place in romance and mysticism.
Just as with its multi-faceted scent, the rose is more than one colour, and neither is it particularly European. Traces of rose wreaths have been found in ancient Egyptian tombs.  Unlike stone or metal dried plants life rarely survives time and the origin of rose usage is rare before the Classical period. The oldest painting of a rose was found in a wall fresco from the Minoan civilisation in Knossos created between 1900 and 1700 BCE. Traces of the original colours can be seen both a yellow tinge and a pink. 

The classical mythology of Europe relates the story of the goddess Aphrodite and Adonis. Aphrodite was the goddess of love, lust, beauty, pleasure, passion and fertility. She was an immortal, one of the Olympian gods. The origins of her worship preceded her Greek myth, for she was the Phoenician Ishtar, whose cult was based on the Sumerian cult of Inanna, Queen of heaven.
Aphrodite’s symbol became the red rose after her mortal lover Adonis, was gored in the groin by a wild boar so symbolising his loss of masculinity and his life.  Aphrodite ran to her lover but too late to save him for tripping upon a rose runner she pricked her foot on the thorns of a white rose and stained the flower with her blood; whereupon the rose turned red. The red rose became the symbol of passionate love.

Classical Greece was very well acquainted with the rose so clearly the rose with its fragrant uses must have predated the classical period. In the Iliad the story is told of Hector after his death at the hands of Achilles was anointed with rose oil. At the time only maceration of rose petals were known so many tons of roses had to be produced to make an effective rose scented oil. This implies a large agricultural industry.

According to the same Iliad Aphrodite washed her skin with rose oil by day and night! Rose cultivation must have been in vogue for the Greek historian Herodotus records King Midas of Phrygia having a cultivated rose of sixty petals. It was Sappho the Greek poetess writing in Lesbos in the 7th century BCE who termed the Rose ‘Queen of Flowers’ writing, ‘The rose each ravished sense beguiles’. It was the Romans however that could be called mad about the rose.

In ancient Rome roses were everywhere and so to support this demand Rose growing had to be extensive. Rose unguents and cosmetics were common, rose filled pillows, wreaths for all manner of occasions, raining rose petals upon guests, and Mark Antony’s fleet had its sails scented with rose water. Extravagance was the moment the emperor Nero spent over a one hundred and fifty thousand euro to cover the beach at Baiae near Naples.

As perfumers we might take notice of the varieties chosen and the places where the roses were grown and cultivated. We would look to modern Palestrina southeast of Rome and the Nile Delta as well as in North Africa modern Algeria and Morocco. What remains a mystery is how the rose petals coming by sea from North Africa, is how the flowers apparently remained fresh and unspoiled.
The most likely species of rose eventually providing the cultivars of the Greeks and Romans is from the wild Rosa Gallica. Once the Dark ages descended upon Europe it was not until the Crusaders returned that the finer things of life caught hold again. Thibault the IV, Count of Champagne and troubadour returned with the rose variety Gallica ‘officinalis’ that has given us the Gallica roses even providing rose varieties today. It was notable for its scent.

The town of Provins once the capital of the Counts of Champagne became the centre of the rose petal industry. Midsummer flowering these are the large, flattish double flowered roses loved by the Empress Josephine at Malmaison where 160 varieties were known.

If the crusade reinvigorated the interest in the beauty and the scent of roses it was from Persia that much of the rose romance originates. Persian carpets, paintings and poetry are suffused with roses. We should well remember that Avicenna the famed physician is described as the father of aromatherapy. Certainly the art of distillation was known and used to produce the famous rose water. As Islam took hold in Persian society the symbolism of the rose was maintained in the Muslim religion. The famous poet Omar Khayyám was reputed to have rose growing on his grave from which seed was collected and cultivated in the famous London Kew gardens and is still grown today.

This Persian rose we are now talking about Rosa damascene, the Damask rose or sometimes as Bulgarian rose or Turkish rose. The damascene is highly fragrant and was cultivated in mists of time. Unlike Gallica which has a single flowering period damascene has a secondary type called semperflorens which has a longer flowering period.  Iran, Bulgaria and Turkey are the most prolific producers of rose oil from the different cultivars of Rosa × damascene.
The rose variety Kazanlik, grown in Bulgaria in the Rose Valley region, produces the finest distilled otto or pure rose oil. Under the Ottoman Empire, and especially from the 19th century Bulgaria has become the world leader in manufacturing rose otto.  Whilst the emphasis might be upon the scent rose has a long history as an apothecary standby as an anti-inflammatory and antioxidant which makes it ideal for skincare benefits.

Modern genetics suggest that this prolific scented Damask rose has R.Gallica in its parentage combined with Rosa Moschata the Musk rose. The musk rose’s origins are a mystery. It has never been found in a truly natural state. Whilst R.Damascena is collected in early morning when its scent is best the Musk rose scent travels far and is most potent at dusk. The fragrance is not found in its petals but its stamens. In his work ‘Of Gardens’, the English philosopher Francis Bacon declared the musk rose second only to violets in yielding ‘the sweetest smell in the air’.

There are five classic roses that make up what is known as the eldest group of cultivated roses. They are Gallica, Damask, Alba, Centifolia, and Musks. R. Alba maintains the sweetness of aroma expected by these older roses and it became famous for its choice as the White Rose of the House of York during the English wars of the Roses for the English crown succession. The house of Lancaster sported the red rose., the R.Gallica officinalis.

Sometimes because the town of Provins sounds like the region of Provence the two names are confused. The Provence rose, is Rosa Centifolia, meaning the rose with a hundred petals. This rose is also known as the cabbage rose or Rose de Mai and familiar as the source of many rose absolutes. Its parentage includes R.Damascena hence the fragrance.

If we guess that R.Moschata originated on the eastern end of the Himalayas we can look further east to China. China has its own set of cultivars and as we are discovering with roses their origins are obscure, not fully known.  Roses as we would understand them, are not pictured in China before the tenth century unlike the Chrysanthemum which is seen from earliest times. Roses do not feature in Chinese mythology and have no great prominence in herbals although cultivated for some centuries.

In Europe it appears that roses were mostly grown for their petals or as extracts in the form of maceration, distillations and waters. Fragrance and perfume then were the most prominent or desirable features. Whilst roses were in themselves beautiful, they were not cultivated in the same way as today which now emphasises colour and flower shape as most significant. This change came with the introduction of what came to be known as China roses.

China was a closed country to Europeans for many years. The Portuguese were the first to establish a trading post in Macao and later came the English East India Company who established a monopoly of trade from Macao and Canton. Foreigners were restricted from entering inland so no great plant hunters or botanical expeditions took place before 1870. Instead, a few different roses trickled through, mostly small flowered with little or no scent but with a perpetual flowering time. By the 19th century four stud types of China roses had been established including yellow rose and those with a scent of tea.  

In the modern world Hybrid Tea roses are the biggest and most popular group of roses commercially sold. As noted above shape or form colour and texture has taken over as pride of place in choice. Scent is secondary and not outstanding as with the older varieties. The question we could ask is what does a rose smell like?
There is no distinct rose smell. Rose not only has a variety of cultivars and species but also the same gamut of smells. Many odours can be found like the smell of green tea, honey, lemon or citrus, moss, fruit, or like other flower species such as violets, or clover even hay. The smell that majority of people associate with roses belongs to the Damask rose, R.Damascena, thought to be by some the most fragrant of rose species. The smell of the Damask rose is recognised as the standard in the fragrance industry for real or pure rose otto.
Picture
The absolute is often termed Rose Centifolia Absolute or Moroccan rose. This has a sweet honey note turning with spicy, citrus, waxy fatty amber resinous feel. I think it quite unlike the Damask rose.  Morrocco too has its The Valley of Roses at the foot of the High Atlas Mountains, where the mountains meet the Dadès Valley. The valley supports many rose varieties including R.Damascena but with a bias toward R.Centifiolia. The main local produce, handpicked, goes to the production of rose hydrolat and concrete. The conversion to absolute is mostly carried out in Spain or France.

There are many variations in the smell of absolutes and an absolute from perfumery raw material suppliers such as Firmenich may not necessarily correspond to say that of IFF or Albert Vieille. There are many great names that supply excellent natural rose extracts and essences. Unfortunately the main constituents such as phenylethyl alcohol, citronellol and geraniol are easily replicated and due to cost of the original natural sources most rose fragrances are synthetic.

One now famous rose grower in the UK, David Austin bred the English Rose. As French growers since the time of Malmaison had maintained their traditional fragrant heritage the market had moved to the world of Hybrid Teas. David Austin began some now 60 years ago to reverse this trend. The most famous rose for fragrance from this grower is called Gertrude Jekyll and now small lots of this rose are on offer as either otto or macerates. If a gardener, the choice is now over 200 varieties with a highly fragranced selection of over seventy which can be distilled for their fragrance with their subtle differences.

It is a joy to see that artisan distillers and producers are beginning to turn to these small batch productions which can provide the natural perfumer with a new source of inspirations and ideas. Instead of the traditional fields of pink Kazanlik variety it is also a visual joy now to see the colours of white, cream, cerise, yellow, peach and red contributing the sensory experience of the Queen of Heaven, the mystic rose.
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ENFLEURAGE TO CAPTURE THE SOUL OF FLOWERS

31/5/2021

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Rose enfleurage
THE POWER OF THE RAW MATERIAL AND THE ART OF REDISCOVERING
​THE ORIGINS OF NATURAL PERFUMERY.

A sentimental introduction to the extraction of raw materials.
by Andrej Babicky, Certified Natural Perfumer
​The natural raw materials are obtained through different extraction methods: from distillation, pressing, maceration, washing with solvents to enfleurage. Each of these extraction techniques should correspond to precise criteria to be both repeatable and sustainable: the raw material should allow to obtain a qualitatively and quantitatively high yield, be easily executable, sustainable, and have a low production cost. For those who could produce raw materials on their own, some of these factors are only relatively important, allowing them to engage in the extractions that are commercially unavailable or expensive both in terms of the availability of the raw material and the time spent in processing (for example violet enfleurage). 
Violet enfleurage
Enfleurage is one of my favorite methods as it manages to capture the ephemeral soul of a flower, its aromatic breath by entangling it. I find there is something magical and alchemical in this process. 
It is a long, demanding technique and requires constant access to fresh raw material, but for those like me who have a garden where they grow some fragrant plants, or a balcony or just a window, it could be an experiment to try. In my opinion in this way, through cultivation and extraction, we enter a more intimate and personal relationship with the raw material; we get to know it and we are often pleasantly surprised by the result obtained.
Enfleurage is a historical extraction procedure, developed in the Grasse region. Nowadays it is a technique almost completely disappeared, replaced by extraction through solvents. In recent years, a revival of this technique can be observed by natural perfumers who rediscover its potential and magic.
Enfleurage is used for the processing of flowers that contain low quantities of perfumed raw material or that are too fragile for other types of extraction or that can be altered with heat (jasmine, violet, lilac, narcissus, etc.). The basic principle lies in the ability of a fat base to absorb volatile odorous substances from the flowers/plants it comes into contact with. Historically, the fat was made up of animal or mineral fats or a mixture of these.
 
We know two types of enfleurage: hot and cold. Hot enfleurage was used for flowers that tolerated the high temperatures necessary to maintain liquid fat such as broom or rose.
Roses enfleurage
Cold enfleurage, on the other hand, consists of the application of a thin layer of fat on glass plates enclosed by a frame (chassis).
The grease is spread on both sides of the chassis. Fresh flowers are placed on one side in contact with the fatty part. A new chassis is superimposed on top and consequently prepared and so on. An extraction chamber is created between the two plates where the odorous molecules are trapped in the fatty part: on the one hand, due to the direct contact of the material with the fat, on the other hand, the more volatile molecules are trapped in the overlying layer. The exhausted flowers are removed from the chassis (defleurage) and replaced with fresh flowers which this time are placed on the other side of the frame. This process is repeated several times (around 30). Saturated fat is called pommade and is marked by the number of cycles performed. The pommade is further treated by washing with ethyl alcohol, which dissolves the essence and part of the fats. The residual oils and fats can be eliminated through cooling and filtration. The extract can be then distilled at low temperatures to eliminate alcohol, or the alcohol can be left to evaporate to obtain an absolute. The extract thus obtained is called absolue ex enfleurage.
 
As I have already mentioned above, enfleurage, despite being laborious and time-consuming, is one of my favourites due to its magical ability to give us the olfactory profile of a flower as if it were a fingerprint.
I approached this technique because I wanted to capture the characteristic scent of wild violets, which I could not achieve with other types of extractions or replicate through accords. As a base, I have tried several types of vegetable butters and oils with a high melting point and long shelf life. My favourite, both for its durability and its easy availability, is deodorized coconut oil. I had chosen to use it without further additions of other oils or waxes as the temperatures during the period of violets flowering do not exceed 20 degrees. For the occasion, I simplified the classic enfleurage process using oven dishes and glass containers instead of chassison which I spread a thin layer of semi-solid coconut oil. The flowers were left on the grease overnight. After about 80 changes of fresh flowers, I got a faintly scented pommade of violet. You can imagine my disappointment because I was hoping to get a usable extract right away. Unfortunately, this was not the case. After some research, I decided to freeze the pommade of violets and to continue the same process the following year. I would have liked the new flowering season of violets to arrive immediately to be able to continue but I had to wait more or less patiently trying to refine my technique. With 200 refills in total, I got around 600 grams of perfumed pommade that I keep as a memento of this first experiment.
With time and various tests, I discovered that enfleurage can be done almost all year round, as long as you have fresh flowers available. Depending on the external temperatures, I added between 1 and 3% beeswax or rice wax to the coconut oil to make it more solid.
stephanotis enfleurage
Enfleurage, more than any other method of extraction, gives the possibility to experiment and explore. For fun I started to co-enfleurage different types of flowers to obtain a more complex, rich, and multifaceted pomade, mixing jasmine of different varieties, gardenias and plumeria flowers, Stephanotis and Cestrum, jasmine and banana leaf, or roses and tomato leaf. 
In addition to an experiment, it is also a game: to capture the decadent fragrance of dying lilies, I used slightly withered Casablanca lilies intending to catch their last breath. For each flower, I had to remove the pistils because I discovered to my expense that they dyed the fatty base yellow. With 60 refills I got an extremely fragrant pomade. Over time I began to incorporate different types of raw materials into the pomade by often playing with unrefined coconut oil with its tropical aroma and using it as a base for enfleurage of gardenia or plumeria flowers along with bourbon vanilla pods. The finely ground benzoin resin together with the iris powder incorporated into the pomade for Jasmine sambac enfleurage to create new odors or recreate complex and unique bouquets.
Absolue from enfleurage
The manufacturing process has not changed much since my first experiment with violets. I continue to use glass or ceramic containers instead of the classic chassis, coconut oil, if necessary combined with vegetable waxes or beeswax. The pomade is always spread in quantities of about 300 grams per medium-sized container, the flowers are changed more or less often depending on the flower or the result I want to obtain, never exceeding 24 hours to avoid the onset of rot and mould. The pomade is then closed in glass jars with alcohol in a ratio of 1: 1, slightly heated to make the fat liquid, and mixed often. When the alcohol is saturated with the perfume, the mix is frozen and filtered. The extract thus obtained can be used without further processing or by letting the alcoholic part evaporate to obtain an absolute. The residual fat is used in the production of soaps. 
Pomade not washed with alcohol can be used as an excellent base for solid perfumes.
 
Some of the enfleurage created remains soaked in alcohol for several months, especially those created in the summer as I do not like to heat the pomade to keep it in a liquid state. Many of these are experiments without ever using them in a composition. They allow me to study a certain type of raw material and its behavior during extraction in a practical way. The time has not yet arrived, but I hope that in the future I will be able to create a perfume entirely made from raw materials extracted by myself that come from my garden and the surrounding area.
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